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DSIP — research-grade lyophilized peptide vial from Peptide.Express, ≥99% HPLC purity
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DSIP — Delta Sleep-Inducing Peptide | Endogenous Nonapeptide (WAGGDASGE) for Sleep Architecture Research

Research-Grade Compound

DSIP (delta sleep-inducing peptide) is an endogenous nonapeptide with the sequence Trp-Ala-Gly-Gly-Asp-Ala-Ser-Gly-Glu (WAGGDASGE), first isolated in 1977 from the cerebral venous blood of rabbits undergoing induced slow-wave sleep. Molecular formula C35H48N10O15, molecular weight 848.8 Da, CAS 62568-57-4.

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≥99% by HPLCLC-MS/MS VerifiedCoA Every BatchIn-Vitro Research Use Only

What is DSIP?

DSIP (delta sleep-inducing peptide) is an endogenous nonapeptide with the sequence Trp-Ala-Gly-Gly-Asp-Ala-Ser-Gly-Glu (WAGGDASGE), first isolated in 1977 from the cerebral venous blood of rabbits undergoing induced slow-wave sleep. Molecular formula C35H48N10O15, molecular weight 848.8 Da, CAS 62568-57-4.

The name records the assay that found it, not a mechanism anyone has since pinned down. Monnier and Schoenenberger separated a fraction of blood from sleeping animals, transferred it to recipient animals, observed an increase in delta-frequency EEG activity, and named the responsible peptide accordingly. That is a functional definition from a single preparation, and nearly fifty years later it remains the strongest claim in the compound record.

DSIP is found endogenously in the hypothalamus, limbic structures, pituitary and plasma, and it crosses the blood-brain barrier — a property uncommon among peptides of this size and part of why it stayed interesting after the sleep findings proved hard to replicate. What DSIP does not have is a receptor. No DSIP receptor has been cloned or characterised, no consensus binding site exists, and every mechanism described below is an association rather than a pathway. Among the compounds in the Peptide.Express catalog, DSIP is the one where the gap between name recognition and characterised pharmacology is widest.

How Does DSIP Work? Mechanism of Action

Start with what is absent, because it governs how everything else should be read: there is no identified DSIP receptor. Without a binding target, the reported effects are observations of what happens after administration, not descriptions of a signalling cascade. Any account of DSIP mechanism that reads as confidently as a GPCR mechanism is overstating the evidence.

On sleep architecture, the original finding was increased delta-frequency (slow-wave) EEG power in rabbit and rat preparations. Replication across laboratories has been uneven — some groups reproduced an effect on slow-wave activity, others found none, and differences in species, administration route and EEG scoring criteria account for some but not all of the divergence. What DSIP does not appear to be is a conventional sedative: it does not behave as a GABA-A receptor agonist and does not produce the pharmacological signature of benzodiazepines or barbiturates in standard assays. Whatever it modulates, it modulates upstream of the classical sedative targets.

Outside sleep, the reported associations are broad and individually thin. Attenuation of CRF-induced corticosterone release appears in stress-axis models, though the same evidence found no effect on ACTH-induced corticosterone release specifically. Effects on LH secretion, interactions with somatostatin signalling, opioid-system interactions in analgesia preparations, and antioxidant activity have all been described. Each of these rests on a small number of studies rather than a replicated body of work, and none has been tied back to a receptor.

Blood-brain barrier transport is the mechanistic finding that has held up best. DSIP crosses into the CNS, which makes it usable in designs where a systemically administered compound needs to reach central tissue. Against that, plasma stability is poor — DSIP is degraded rapidly by circulating peptidases — so the exposure achieved after systemic administration is brief and hard to characterise. Researchers designing DSIP studies should treat both the transport and the degradation as first-order variables rather than background details.

Research Applications of DSIP

Sleep Architecture and EEG Research

  • Delta-power quantification: spectral analysis of slow-wave EEG activity in rodent and rabbit preparations is the endpoint the compound was originally named for.
  • Sleep-stage transition mapping: measuring changes in the distribution of sleep stages rather than total sleep duration is the more informative design given the inconsistency of the earlier literature.
  • Sedative-mechanism exclusion: running DSIP alongside a GABA-A agonist arm distinguishes slow-wave modulation from general sedation.

Neuroendocrine and Stress-Axis Models

  • Corticotropin-releasing signalling: attenuation of CRF-induced corticosterone release is among the more frequently reported non-sleep effects, though from a small evidence base, with no effect observed on ACTH-induced output specifically.
  • Gonadotropin interaction studies: reported effects on LH secretion place DSIP loosely alongside the HPG-axis compounds, without a mechanism connecting the two.
  • Opioid and somatostatin system interaction: analgesia and neuroendocrine preparations examining whether DSIP effects are blocked by opioid antagonists.

Blood-Brain Barrier Transport and Peptide Stability

  • CNS penetration studies: DSIP is used as a reference compound in peptide transport research because it crosses the barrier at a measurable rate.
  • Plasma degradation kinetics: rapid peptidase cleavage limits systemic exposure, and characterising that decay is necessary before any dose-response interpretation.
  • Analog stabilisation work: modified DSIP sequences are studied primarily to extend plasma half-life rather than to alter target engagement, since no target has been identified.

DSIP vs Melatonin

FeatureDSIPMelatonin
Chemical classNonapeptide (WAGGDASGE)Indoleamine, tryptophan-derived small molecule
Molecular weight848.8 DaSmall molecule, far below peptide range
Source of discoveryCerebral venous blood of sleeping rabbits, 1977Pineal gland extract, 1958
ReceptorNone identifiedMT1 and MT2 G protein-coupled receptors
Primary research framingSlow-wave (delta) EEG powerCircadian phase shifting and entrainment
Endogenous rhythmNot establishedStrongly circadian, suppressed by light exposure
Evidence baseSparse and inconsistently replicatedLarge, replicated across species and laboratories
Regulatory status (US)Research compound, no approvalMarketed as a dietary supplement

These two get filed together in consumer discussion under the heading of sleep compounds, and mechanistically that is a category error — which is exactly why the comparison is worth drawing. Melatonin has cloned receptors, a characterised circadian role and decades of replicated work behind it. DSIP has a name derived from one 1977 preparation and no identified receptor at all. A study design that treats them as members of the same pharmacological class starts from a false premise.

DSIP Technical Specifications

Technical specifications for DSIP, including molecular data, purity standard, testing methods and storage requirements.
Compound NameDSIP (delta sleep-inducing peptide)
Common SynonymsDelta sleep-inducing peptide, delta sleep peptide, DSIP peptide
ClassificationEndogenous linear nonapeptide
Amino Acid SequenceTrp-Ala-Gly-Gly-Asp-Ala-Ser-Gly-Glu (WAGGDASGE)
Amino Acid Count9 (nonapeptide)
CAS Number62568-57-4
Molecular FormulaC35H48N10O15
Molecular Weight848.8 Da
Receptor TargetNone identified — no DSIP receptor has been cloned or characterised
Blood-Brain BarrierCrosses the barrier at a measurable rate
Endogenous DistributionHypothalamus, limbic structures, pituitary, plasma
First Isolated1977, from cerebral venous blood of rabbits in induced slow-wave sleep
Purity≥99% by HPLC
Purity ConfirmationLC-MS/MS molecular weight verification
Endotoxin TestingLAL (Limulus Amebocyte Lysate) method
Physical FormLyophilized powder
AppearanceWhite to off-white powder
ReconstitutionBacteriostatic water or sterile 0.9% sodium chloride
Storage (lyophilized)-20°C, desiccated, protected from light
Storage (reconstituted)2–8°C, use within 14–28 days
Shelf Life24 months from manufacture (lyophilized)
Testing MethodsHPLC, LC-MS/MS, LAL Endotoxin
DocumentationCertificate of Analysis (CoA) per batch
FDA StatusNot approved for human use
Intended UseIn-vitro laboratory research only

How to Reconstitute DSIP for Research

DSIP is a small, highly polar peptide with two acidic residues, and it dissolves quickly — often within 30 seconds of gentle swirling. The tryptophan at position 1 makes the reconstituted solution light-sensitive, so keep the vial covered rather than parked under bench lighting.

  1. Allow the vial to reach room temperature before opening.
  2. Draw the calculated volume of bacteriostatic water. For a 10 mg vial, 2 mL yields 5 mg/mL and 5 mL yields 2 mg/mL.
  3. Swab the septum with alcohol and allow 30 seconds to dry.
  4. Inject the diluent slowly against the inner vial wall.
  5. Swirl gently until dissolution is complete. DSIP goes into solution faster than most peptides in this catalog — do not add agitation it does not need.
  6. Confirm the solution is clear and colorless with no visible particulate.
  7. Label with the reconstitution date and resulting concentration.
  8. Store at 2–8°C, protected from light, and use within 14–28 days.

Diluent: bacteriostatic water for peptide reconstitution. Full protocol: step-by-step peptide reconstitution guide. Concentration maths: peptide reconstitution calculator.

Frequently Asked Questions — DSIP

What is DSIP peptide?

DSIP is an endogenous nonapeptide — sequence Trp-Ala-Gly-Gly-Asp-Ala-Ser-Gly-Glu, molecular weight 848.8 Da, CAS 62568-57-4 — isolated in 1977 from the cerebral venous blood of rabbits in induced slow-wave sleep. It is supplied by Peptide.Express as a lyophilized powder for in-vitro laboratory research only.

What does delta sleep-inducing peptide do in research models?

The original and defining observation was an increase in delta-frequency EEG power in animal sleep preparations. Replication has been uneven across laboratories, and the compound has also been reported to affect ACTH and LH release, interact with opioid and somatostatin signalling, and show antioxidant activity. Each of those sits on a small evidence base. The honest summary is that DSIP has a well-known name and a poorly characterised pharmacology.

What is DSIP mechanism of action?

Not established. No DSIP receptor has been cloned or characterised, so there is no binding-site account to give. What exists is a set of downstream observations from administration studies, which is a categorically weaker form of evidence than a receptor-linked mechanism. Researchers should design around that gap rather than write past it.

Is DSIP related to GABA or standard sedative pathways?

It does not appear to be. DSIP does not act as a GABA-A receptor agonist and does not produce the pharmacological profile of benzodiazepines or barbiturates in standard assays. Whatever modulation it exerts on sleep-regulatory circuits operates through something other than the classical sedative targets.

Does DSIP cross the blood-brain barrier?

Yes — that is one of the better-supported findings about it, and part of why the compound remained of interest after the sleep data proved inconsistent. It is used as a reference compound in peptide transport research for that reason.

What is the difference between DSIP and melatonin?

Almost everything except the topic they get discussed under. Melatonin is a small indoleamine with two cloned receptors, MT1 and MT2, a strong endogenous circadian rhythm and a large replicated literature on phase shifting. DSIP is a nonapeptide with no identified receptor, no established endogenous rhythm and a sparse, inconsistently replicated evidence base. Grouping them as sleep compounds is a consumer-facing convenience, not a pharmacological classification.

Why is DSIP considered under-characterised?

Because the basic pharmacological facts are missing. Nearly five decades after isolation there is no receptor, no consensus signalling pathway, and no consistently replicated dose-response relationship for the effect it was named after. Meanwhile the compound has a high public profile relative to its evidence base. Both of those things are true at once, and a research protocol should be built around the first rather than the second.

How stable is DSIP in plasma?

Poorly. It is cleaved rapidly by circulating peptidases, which means systemic administration produces brief and difficult-to-characterise exposure. Analog work on DSIP has focused largely on extending plasma half-life for exactly this reason.

Where is DSIP found endogenously?

In the hypothalamus, limbic structures, pituitary and plasma. Its presence across both central and peripheral compartments is consistent with the blood-brain barrier transport findings.

What purity standard and testing does Peptide.Express apply to DSIP?

≥99% by reverse-phase HPLC with LC-MS/MS confirming the 848.8 Da mass, LAL endotoxin testing, and visual QC. Independent third-party testing with a batch-specific Certificate of Analysis per lot.

How should DSIP be stored before and after reconstitution?

Lyophilized: -20°C, desiccated and protected from light, stable for 24 months from manufacture. Reconstituted: 2–8°C, light-protected, used within 14–28 days. Do not freeze the reconstituted solution.

Where is the Certificate of Analysis for DSIP?

On this page and in the Peptide.Express lab results library. Each CoA is batch-specific and lists HPLC purity, LC-MS/MS mass confirmation, endotoxin result, testing laboratory and test date.

Research References

  1. Schoenenberger GA, Monnier M. Characterization of a delta-electroencephalogram(-sleep)-inducing peptide. Proc Natl Acad Sci U S A. 1977. Read Schoenenberger and Monnier's 1977 isolation and characterization of DSIP
  2. Banks WA, Kastin AJ, Coy DH. Evidence that [125I]N-Tyr-delta sleep-inducing peptide crosses the blood-brain barrier by a non-competitive mechanism. Brain Res. 1984. Read Banks, Kastin and Coy on DSIP blood-brain barrier transport
  3. Graf MV, Kastin AJ, Coy DH, Fischman AJ. Delta-sleep-inducing peptide reduces CRF-induced corticosterone release. Neuroendocrinology. 1985. Read Graf et al. on DSIP's effect on CRF-induced corticosterone release

All products are sold for in-vitro laboratory research use only. Not intended for human consumption, clinical use, or veterinary use. Peptide.Express makes no medical claims. Consult the published literature for research application guidance.

Further Reading